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What are the physical properties of methyl 4-iodobenzoate?
Ethyl 4-hydroxybutyrate is an organic compound. Its physical properties are as follows:
Viewed, it is often a colorless to light yellow transparent liquid, pure with a clear state, refracted under light, if it is full of autumn water, without the slightest disturbance of impurities.
Smell it, exudes a pleasant fruity aroma, just like a ripe fruit, light and fragrant, fresh and elegant, its taste is faint, lingering in the nose, giving people a sense of comfort.
When it comes to boiling point, it is about 180-184 ° C. When placed in a heating device, the temperature is approaching this area, the thermal movement of the molecules intensifies, breaking free from the shackles of the liquid phase, and turning into curling steam. This boiling point makes it possible to realize the conversion of gas and liquid under specific temperature conditions, and is an important reference index in chemical operations, separation and purification.
Its melting point is about -43 ° C. When the temperature is low to this limit, the activities of molecules gradually slow down, embrace each other, and condense from the flowing liquid state to the solid state, just like time solidifies, showing a different form.
In terms of density, it is about 1.03 - 1.04 g/cm ³. Compared with water, it is slightly heavier than water. If it is placed in the same container as water, it will be like a stable person, quietly sinking at the bottom, showing its unique density characteristics.
In terms of solubility, it can be soluble in organic solvents such as ethanol and ether. In the embrace of organic solvents, it is like a fish entering water and can blend with it to form a uniform system. However, the solubility in water is limited, just like the incompatibility of oil and water, it can only be slightly soluble in water, reflecting its affinity for different solvents.
What are the chemical properties of methyl 4-iodobenzoate?
Benzyl 4-bromobenzoate is an organic compound. It has the following chemical properties:
Nucleophilic Substitution Reaction: Among this compound, the bromine atom has good activity and can react with many nucleophiles. For example, under alkaline conditions, it can react with alcohol nucleophiles to generate corresponding ether compounds. In this process, the oxygen atom of the nucleophilic reagent attacks the carbon atom connected to the bromine atom, and the bromine ion leaves to complete the substitution. The reaction mechanism is to provide electron pairs for the nucleophilic reagent to bond with the carbon atom lacking electrons in the substrate to achieve substitution.
Hydrolysis Reaction: Under the catalysis of acid or base, the ester bond of 4-bromobenzoate can be hydrolyzed. In acidic conditions, the proton first combines with the carbonyl oxygen atom in the ester group to enhance the positive electricity of the carbonyl carbon. Water molecules attack the carbonyl carbon, and after a series of intermediates, 4-bromobenzoic acid and benzyl alcohol are finally formed. Under basic conditions, the hydroxide ion directly attacks the carbonyl carbon to form 4-bromobenzoate and benzyl alcohol. The reaction is more complete because the generated carboxylate is highly stable.
Reduction reaction: The bromine atom in the molecule can be reduced. For example, the use of certain metal hydrides, such as lithium aluminum hydride (LiAlH), can provide hydrogen negative ions, attack the bromine atom, and replace the bromine atom with the hydrogen atom to obtain the corresponding reduction product. In this reaction, lithium aluminum hydride is a strong reducing agent, and the negative hydrogen ion acts as a nucleophilic reagent to replace the bromine atom.
In addition, its benzyl moiety also has certain activity. Under specific conditions, the hydrogen atom on the benzyl group can be replaced by other groups. For example, in the presence of light or an initiator, it can undergo a free radical substitution reaction with halogen elements. The process is that the halogen forms a free radical under the action of light or an initiator, captures the hydrogen atom on the benzyl group, and generates a benzyl radical. The benzyl radical reacts with the halogen element to obtain the benzyl halogen product. These chemical properties of 4-bromobenzoate make it widely used in the field of organic synthesis and can be used to prepare a variety of organic compounds.
What are the main uses of methyl 4-iodobenzoate?
Methyl 4-carboxybenzoate, also known as paraben methyl ester, is a commonly used chemical compound. Its main use is wide, and it is important in many fields.
In the field, it is often used as an antiseptic agent. The product needs to be properly stored to prevent the growth of microorganisms and cause the growth of the product. Methyl 4-carboxybenzoate can effectively inhibit the growth of microorganisms such as bacteria and bacteria, and ensure the safety of the product in the valid period. For example, in liquids, ointments, etc., it is often added to extend the shelf life of the product to ensure the safety of patients.
In chemical products, it is the same as the important function of anti-corrosion. Chemical products are rich in various ingredients and are easily contaminated by microorganisms. Adding 4-methylbenzoate can prevent the chemical product from producing a smell, such as milk, etc. due to the reproduction of microorganisms during the use process, and the quality of the chemical product can be determined, so that the consumer can use it with peace of mind. Such as creams, lotions, washing water and other chemical products have their own figures.
In food engineering, it is also used as food preservative. The storage of food requires a certain period of time to prevent food rot and ensure food safety. Methyl 4-phenylbenzoate can inhibit the microbial activity in food and extend the shelf life of food. For foods such as food ingredients, vegetables, cakes, etc., adding this product in an amount can not only maintain the taste of food, but also ensure that the amount of food in the circulation and sales process is not affected.
Therefore, methyl 4-alkyl benzoate, with its excellent anti-corrosion properties, plays a crucial role in many industries such as chemicals, food, etc., to ensure product safety, safety, and extended shelf life.
What are the synthesis methods of methyl 4-iodobenzoate?
4-Methyl benzoate and methylparaben are commonly used chemical compounds. They are used in various fields such as food, chemicals, etc., and are used as anti-corrosion agents. There are many methods for their synthesis, which will be described in this article.
First, the raw material of methanol and sulfuric acid are used as catalysts to carry out esterification reaction. The inverse formula is as follows:
methylbenzoic acid + methanol $\ {< = > [sulfuric acid] [plus]} $4-methylbenzoic acid + water
This reaction is mature, but the sulfuric acid corrosion is low, and it is easy to cause corrosion.
Second, the use of solid acid catalysis to replace sulfuric acid. Such as cross-lipids, molecules, etc., this catalyst has high activity, good performance, easy separation, weak corrosion, etc., which can effectively overcome the drawbacks of sulfuric acid and improve the reaction efficiency.
Third, with the raw material of benzoic acid, dimethyl carbonate is methylated. Dimethyl carbonate is chromogenic, with low toxicity and environmental friendliness. In this reverse system, under the action of suitable catalysis, dimethyl carbonate of benzoic acid is reversed to generate 4-methyl benzoate, which fits the concept of chromogenic, and has a good application prospect.
Fourth, enzyme-catalyzed synthesis method. The use of biological enzymes such as lipase as catalysis can promote the esterification of methyl benzoate and methanol under the combination of antibodies. Enzyme catalysis has the characteristics of high reliability, antibodies, and environmental friendliness, etc. However, the cost of enzymes is high, and the qualitative quality is poor, which limits its use in large-scale molding.
Of course, the synthesis methods of methyl 4-benzoate have their own shortcomings. In the production process, it is necessary to choose the best method according to the needs of the product.
What are the precautions for the storage and transportation of methyl 4-iodobenzoate?
4-Benzyl-2-oxo-4-phenylbutyrate benzyl ester should pay attention to the following matters during storage and transportation:
First, when storing, it should be found in a cool, dry and well-ventilated place. This compound is quite sensitive to temperature and humidity, and high temperature and humidity can easily cause it to deteriorate. Therefore, the warehouse temperature should be controlled below 20 ° C, and the relative humidity should be maintained within 60%. If placed in a humid environment, it may cause hydrolysis reactions and damage product quality.
Second, it must be stored in isolation from oxidants, acids, bases, etc. Because of its active chemical properties, contact with the above substances can easily trigger chemical reactions, or cause combustion, explosion and other dangerous situations. For example, when it encounters a strong oxidizing agent, it may react violently and release a large amount of heat energy.
Third, ensure that the packaging is intact during transportation. Strong packaging materials should be used to prevent the packaging from breaking during handling and loading and unloading. And transportation vehicles need to have good shock absorbers and fixtures to avoid damage to the goods due to bumps and collisions.
Fourth, fireworks should be strictly prohibited in transportation and storage places. This compound is flammable to a certain extent, and in case of open flames, hot topics or there is a risk of fire. Therefore, the surrounding area must be equipped with perfect fire protection facilities and equipment, and relevant personnel should be familiar with the fire operation process.
Fifth, the storage area should be equipped with obvious warning signs, indicating the characteristics and danger level of the compound. Transport personnel and warehouse management personnel must be professionally trained to be familiar with their physical and chemical properties, hazard characteristics and emergency treatment measures, so as to respond quickly and effectively in the event of an accident and reduce hazards.